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<h1 id="firstHeading" class="firstHeading mw-first-heading"><span class="mw-page-title-main">Lithiumwolframat</span></h1>
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<div id="mw-content-text" class="mw-body-content mw-content-ltr" lang="de" dir="ltr"><div class="mw-content-ltr mw-parser-output" lang="de" dir="ltr"><table class="wikitable infobox float-right" id="Vorlage_Infobox_Chemikalie" style="font-size:90%; margin-top:0; width:350px;" summary="Infobox Chemikalie">
<tbody><tr>
<th colspan="2" style="background:#FFDEAD; color:#202122;">Kristallstruktur
</th></tr>
<tr>
<td colspan="2" class="hintergrundfarbe-basis" style="text-align:center;"><span typeof="mw:File"></span>
</td></tr>
<tr>
<td colspan="2" style="text-align:center; font-size:80%;"><span style="background:#86E074;border-radius: 12px;color: transparent; width: 12px; line-height:12px;display:inline-block;">_</span> <a href="Lithium" title="Lithium">Li</a><sup>+</sup> <span style="visibility:hidden;">0</span> <span style="background:#8D8A7F;border-radius: 12px;color: transparent; width: 12px; line-height:12px;display:inline-block;">_</span> <a href="Wolfram" title="Wolfram">Wo</a><sup>6+</sup><span style="visibility:hidden;">0</span> <span style="background:#FE0300;border-radius: 12px;color: transparent; width: 12px; line-height:12px;display:inline-block;">_</span> <a href="Sauerstoff" title="Sauerstoff">O</a><sup>2−</sup>
</td></tr>
<tr>
<td><a href="Kristallsystem" title="Kristallsystem">Kristallsystem</a>
</td>
<td>
<p>Trigonal
</p>
</td></tr>
<tr>
<td><a href="Raumgruppe" title="Raumgruppe">Raumgruppe</a>
</td>
<td>
<p><i>R</i><span style="text-decoration:overline">3</span> (Nr. 148)<span style="display:none;">Vorlage:Raumgruppe/148</span><span class="editoronly" style="display:none;"></span>
</p>
</td></tr>
<tr>
<td><a href="Gitterparameter" title="Gitterparameter">Gitterparameter</a>
</td>
<td>
<p>a = 8,888 <a href="%C3%85ngstr%C3%B6m_(Einheit)" title="Ångström (Einheit)">Å</a>, α = 107°78′<sup id="cite_ref-DOI10.1107/S0365110X61000772_1-0" class="reference"><a href="#cite_note-DOI10.1107/S0365110X61000772-1"><span class="cite-bracket">[</span>1<span class="cite-bracket">]</span></a></sup>
</p>
</td></tr>
<tr>
<th colspan="2" style="background:#FFDEAD; color:#202122;">Allgemeines
</th></tr>
<tr>
<td style="width:33%;">Name
</td>
<td>Lithiumwolframat
</td></tr>
<tr>
<td>Andere Namen
</td>
<td>
<ul><li>Dilithiumtetraoxotungstat</li>
<li>Lithiumwolframoxid</li></ul>
</td></tr>
<tr>
<td><a href="Verh%C3%A4ltnisformel" title="Verhältnisformel">Verhältnisformel</a>
</td>
<td>Li<sub>2</sub>WO<sub>4</sub>
</td></tr>
<tr>
<td>Kurzbeschreibung
</td>
<td>
<p>farbloser Feststoff<sup id="cite_ref-Alfa_2-0" class="reference"><a href="#cite_note-Alfa-2"><span class="cite-bracket">[</span>2<span class="cite-bracket">]</span></a></sup>
</p>
</td></tr>
<tr>
<th colspan="2" style="background:#FFDEAD; color:#202122;">Externe Identifikatoren/Datenbanken
</th></tr>
<tr>
<td colspan="2" style="padding:0;">
<table class="mw-collapsible mw-collapsed wikitable" data-expandtext="+" data-collapsetext="−" style="border-top:none; margin:-1px; width:calc(100% + 2px);">
<tbody><tr>
<td style="width:33%;"><a href="CAS-Nummer" title="CAS-Nummer">CAS-Nummer</a>
</td>
<td><span title="Untervorlage eingebunden: CASRN"></span><a rel="nofollow" class="external text" href="https://commonchemistry.cas.org/detail?cas_rn=13568-45-1">13568-45-1</a><span class="editoronly" style="display:none;"></span>
</td>
<td style="background:#FFDEAD; color:#202122; border-top:1px solid #FFDEAD; padding:0.2em 0; vertical-align:bottom; width:5%;">
</td></tr>
<tr>
<td><a href="EG-Nummer" title="EG-Nummer">EG-Nummer</a>
</td>
<td colspan="2">236-978-2
</td></tr>
<tr>
<td><a href="Europ%C3%A4ische_Chemikalienagentur" title="Europäische Chemikalienagentur">ECHA</a>-InfoCard
</td>
<td colspan="2"><a rel="nofollow" class="external text" href="https://www.echa.europa.eu/de/substance-information/-/substanceinfo/100.033.602">100.033.602</a>
</td></tr>
<tr>
<td><a href="PubChem" title="PubChem">PubChem</a>
</td>
<td colspan="2"><a rel="nofollow" class="external text" href="https://pubchem.ncbi.nlm.nih.gov/compound/5062350">5062350</a>
</td></tr>
<tr>
<td style="border-right:1px solid #a2a9b1;"><a href="Wikidata" title="Wikidata">Wikidata</a>
</td>
<td colspan="2"><a href="https://www.wikidata.org/wiki/Q6647973" class="extiw external" title="d:Q6647973">Q6647973</a>
</td></tr></tbody></table>
</td></tr>
<tr>
<th colspan="2" style="background:#FFDEAD; color:#202122;">Eigenschaften
</th></tr>
<tr>
<td><a href="Molare_Masse" title="Molare Masse">Molare Masse</a>
</td>
<td>261,72 g·<a href="Mol" title="Mol">mol</a><sup>−1</sup>
</td></tr>
<tr>
<td><a href="Aggregatzustand" title="Aggregatzustand">Aggregatzustand</a>
</td>
<td>
<p>fest<sup id="cite_ref-Sigma_3-0" class="reference"><a href="#cite_note-Sigma-3"><span class="cite-bracket">[</span>3<span class="cite-bracket">]</span></a></sup>
</p>
</td></tr>
<tr>
<td><a href="Dichte" title="Dichte">Dichte</a>
</td>
<td>
<p>3,71 g·cm<sup>−3</sup> (25 °C)<sup id="cite_ref-Sigma_3-1" class="reference"><a href="#cite_note-Sigma-3"><span class="cite-bracket">[</span>3<span class="cite-bracket">]</span></a></sup>
</p>
</td></tr>
<tr>
<td><a href="Schmelzpunkt" title="Schmelzpunkt">Schmelzpunkt</a>
</td>
<td>
<p>742 <a href="Grad_Celsius" title="Grad Celsius">°C</a><sup id="cite_ref-Alfa_2-1" class="reference"><a href="#cite_note-Alfa-2"><span class="cite-bracket">[</span>2<span class="cite-bracket">]</span></a></sup>
</p>
</td></tr>
<tr>
<td><a href="L%C3%B6slichkeit" title="Löslichkeit">Löslichkeit</a>
</td>
<td>
<p>löslich in Wasser<sup id="cite_ref-Alfa_2-2" class="reference"><a href="#cite_note-Alfa-2"><span class="cite-bracket">[</span>2<span class="cite-bracket">]</span></a></sup>
</p>
</td></tr>
<tr>
<th colspan="2" style="background:#FFDEAD; color:#202122;">Sicherheitshinweise
</th></tr>
<tr>
<td colspan="2">
<table cellspacing="0" cellpadding="2" style="width:100%;">
<tbody><tr>
<td colspan="2" style="text-align:center"><b><a href="Global_harmonisiertes_System_zur_Einstufung_und_Kennzeichnung_von_Chemikalien" title="Global harmonisiertes System zur Einstufung und Kennzeichnung von Chemikalien">GHS-Gefahrstoffkennzeichnung</a></b><sup id="cite_ref-Sigma_3-2" class="reference"><a href="#cite_note-Sigma-3"><span class="cite-bracket">[</span>3<span class="cite-bracket">]</span></a></sup>
<table class="hintergrundfarbe-neutral" style="text-align:center; margin-left:auto; margin-right:auto; display:flex; justify-content:center;">
<tbody><tr>
<td><i>keine GHS-Piktogramme</i>
</td></tr></tbody></table>
<p>
</p>
</td></tr>
<tr>
<td rowspan="2" width="33%" style="border-top:1px #A7A7A7 dashed; border-right:1px #A7A7A7 dashed;"><a href="H-_und_P-S%C3%A4tze" title="H- und P-Sätze">H- und P-Sätze</a>
</td>
<td style="border-top:1px #A7A7A7 dashed;">H: <span title="Untervorlage eingebunden: H-Sätze"></span><i>keine H-Sätze</i>
</td></tr>
<tr>
<td style="border-top:1px #A7A7A7 dashed;">P: <span title="Untervorlage eingebunden: P-Sätze"></span><i>keine P-Sätze</i><sup id="cite_ref-Sigma_3-3" class="reference"><a href="#cite_note-Sigma-3"><span class="cite-bracket">[</span>3<span class="cite-bracket">]</span></a></sup>
</td></tr>
</tbody></table>
</td></tr>
<tr>
<td colspan="2" style="background:#FFDEAD; color:#202122; font-size:80%; text-align:center; line-height:150%; padding:.25em;">Wenn nicht anders vermerkt, gelten die angegebenen Daten bei <a href="Standardbedingungen" title="Standardbedingungen">Standardbedingungen</a> (0 °C, 1000 hPa).
</td></tr></tbody></table><p><span class="editoronly" style="display:none;"></span>
</p><p><b>Lithiumwolframat</b> ist eine anorganische <a href="Chemische_Verbindung" title="Chemische Verbindung">chemische Verbindung</a> des <a href="Lithium" title="Lithium">Lithiums</a> aus der Gruppe der <a href="Wolframate" title="Wolframate">Wolframate</a>.
</p>
<div class="mw-heading mw-heading2"><h2 id="Gewinnung_und_Darstellung">Gewinnung und Darstellung</h2></div>
<p>Lithiumwolframat kann durch Reaktion von <a href="Wolfram(VI)-oxid" title="Wolfram(VI)-oxid">Wolfram(VI)-oxid</a> mit siedender Lösung von <a href="Lithiumcarbonat" title="Lithiumcarbonat">Lithiumcarbonat</a> gewonnen werden.<sup id="cite_ref-R._J._Meyer_4-0" class="reference"><a href="#cite_note-R._J._Meyer-4"><span class="cite-bracket">[</span>4<span class="cite-bracket">]</span></a></sup>
</p>
<div class="mw-heading mw-heading2"><h2 id="Eigenschaften">Eigenschaften</h2></div>
<p>Lithiumwolframat ist ein <a href="Hygroskopisch" class="mw-redirect" title="Hygroskopisch">hygroskopischer</a> farbloser Feststoff, der löslich in Wasser ist.<sup id="cite_ref-Alfa_2-3" class="reference"><a href="#cite_note-Alfa-2"><span class="cite-bracket">[</span>2<span class="cite-bracket">]</span></a></sup><sup id="cite_ref-DOI10.1007/s11581-009-0407-4_5-0" class="reference"><a href="#cite_note-DOI10.1007/s11581-009-0407-4-5"><span class="cite-bracket">[</span>5<span class="cite-bracket">]</span></a></sup> Er kommt in mehreren Modifikationen vor und besitzt bei Raumtemperatur entweder eine <a href="Kristallstruktur" title="Kristallstruktur">Kristallstruktur</a> vom <a href="Phenakit" title="Phenakit">Phenakittyp</a> mit der <a href="Raumgruppe" title="Raumgruppe">Raumgruppe</a> <i>R</i><span style="text-decoration:overline">3</span> (Raumgruppen-Nr. 148)<span style="display:none;">Vorlage:Raumgruppe/148</span><span class="editoronly" style="display:none;"></span>.<sup id="cite_ref-DOI10.1107/S0365110X61000772_1-1" class="reference"><a href="#cite_note-DOI10.1107/S0365110X61000772-1"><span class="cite-bracket">[</span>1<span class="cite-bracket">]</span></a></sup> oder eine <a href="Tetragonal" class="mw-redirect" title="Tetragonal">tetragonale</a> Kristallstruktur die einer verzerrten <a href="Spinell" title="Spinell">Spinellstruktur</a> entspricht mit der Raumgruppe <i>I</i>4<sub>1</sub>/<i>amd</i> (Nr. 141)<span style="display:none;">Vorlage:Raumgruppe/141</span><span class="editoronly" style="display:none;"></span>.<sup id="cite_ref-Evgeni_Tonkov_6-0" class="reference"><a href="#cite_note-Evgeni_Tonkov-6"><span class="cite-bracket">[</span>6<span class="cite-bracket">]</span></a></sup> Bei 40 kBar und 850 °C besitzt er eine <a href="Monoklines_Kristallsystem" title="Monoklines Kristallsystem">monokline</a> Kristallstruktur vom <a href="Wolframit" title="Wolframit">Wolframittyp</a> mit der Raumgruppe <i>C</i>2/<i>c</i> (Nr. 15)<span style="display:none;">Vorlage:Raumgruppe/15</span><span class="editoronly" style="display:none;"></span>.<sup id="cite_ref-DOI10.1016/0022-4596(80)90554-X_7-0" class="reference"><a href="#cite_note-DOI10.1016/0022-4596(80)90554-X-7"><span class="cite-bracket">[</span>7<span class="cite-bracket">]</span></a></sup>
</p>
<div class="mw-heading mw-heading2"><h2 id="Verwendung">Verwendung</h2></div>
<p>Lithiumwolframat wird für die Herstellung von Keramiken mit extrem niedrigen <a href="Sintern" title="Sintern">Sintertemperaturen</a> eingesetzt. Es dient auch als <a href="Katalysator" title="Katalysator">Katalysator</a> für oxidative <a href="Kupplungsreaktion" title="Kupplungsreaktion">Kupplungsreaktionen</a>. Weiterhin wird es zur Herstellung von hochdichten wässrigen Polywolframat (Metawolframat) Lösungen eingesetzt, die zur Trennung von <a href="Mineral" title="Mineral">Mineralen</a> und anderen Feststoffen verwendet werden.<sup id="cite_ref-Alfa_2-4" class="reference"><a href="#cite_note-Alfa-2"><span class="cite-bracket">[</span>2<span class="cite-bracket">]</span></a></sup>
</p>
<div class="mw-heading mw-heading2"><h2 id="Einzelnachweise">Einzelnachweise</h2></div>
<ol class="references">
<li id="cite_note-DOI10.1107/S0365110X61000772-1"><span class="mw-cite-backlink">↑ <sup><a href="#cite_ref-DOI10.1107/S0365110X61000772_1-0">a</a></sup> <sup><a href="#cite_ref-DOI10.1107/S0365110X61000772_1-1">b</a></sup></span> <span class="reference-text">W. H. Zachariasen, H. A. Plettinger: <i>The crystal structure of lithium tungstate.</i> In: <i>Acta Crystallographica.</i> 14, 1961, S. 229, <a href="Digital_Object_Identifier" title="Digital Object Identifier">doi</a>:<span class="uri-handle" style="white-space:nowrap"><a rel="nofollow" class="external text" href="https://doi.org/10.1107/S0365110X61000772">10.1107/S0365110X61000772</a></span>.</span>
</li>
<li id="cite_note-Alfa-2"><span class="mw-cite-backlink">↑ <sup><a href="#cite_ref-Alfa_2-0">a</a></sup> <sup><a href="#cite_ref-Alfa_2-1">b</a></sup> <sup><a href="#cite_ref-Alfa_2-2">c</a></sup> <sup><a href="#cite_ref-Alfa_2-3">d</a></sup> <sup><a href="#cite_ref-Alfa_2-4">e</a></sup></span> <span class="reference-text">Datenblatt <span style="font-style:italic;"><a rel="nofollow" class="external text" href="https://www.alfa.com/de/catalog/43366">Lithiumwolframat</a></span> bei <a href="Alfa_Aesar" title="Alfa Aesar">Alfa Aesar</a>, abgerufen am 5. Juni 2016 <small>(Seite nicht mehr abrufbar)</small>.<span class="editoronly" style="display:none;"></span></span>
</li>
<li id="cite_note-Sigma-3"><span class="mw-cite-backlink">↑ <sup><a href="#cite_ref-Sigma_3-0">a</a></sup> <sup><a href="#cite_ref-Sigma_3-1">b</a></sup> <sup><a href="#cite_ref-Sigma_3-2">c</a></sup> <sup><a href="#cite_ref-Sigma_3-3">d</a></sup></span> <span class="reference-text">Datenblatt <span style="font-style:italic;"><a rel="nofollow" class="external text" href="https://www.sigmaaldrich.com/catalog/product/ALDRICH/400912">Lithium tungstate, 98%</a></span> bei <a href="Sigma-Aldrich" title="Sigma-Aldrich">Sigma-Aldrich</a>, abgerufen am 5. Juni 2016 (<a rel="nofollow" class="external text" href="https://www.sigmaaldrich.com/DE/de/sds/ALDRICH/400912?userType=anonymous">PDF</a>).<span class="editoronly" style="display:none;"></span></span>
</li>
<li id="cite_note-R._J._Meyer-4"><span class="mw-cite-backlink"><a href="#cite_ref-R._J._Meyer_4-0">↑</a></span> <span class="reference-text">R. J. Meyer: <cite style="font-style:italic">Wolfram</cite>. Springer-Verlag, 2013, ISBN 978-3-662-13401-6, <span style="white-space:nowrap">S.<span style="display:inline-block;width:.2em"> </span>208</span> (<a rel="nofollow" class="external text" href="https://books.google.de/books?id=QZSBBwAAQBAJ&pg=PA208#v=onepage">eingeschränkte Vorschau</a> in der Google-Buchsuche).<span class="Z3988" title="ctx_ver=Z39.88-2004&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Abook&rfr_id=info:sid/de.wikipedia.org:Lithiumwolframat&rft.au=R.+J.+Meyer&rft.btitle=Wolfram&rft.date=2013&rft.genre=book&rft.isbn=9783662134016&rft.pages=208&rft.pub=Springer-Verlag" style="display:none"> </span></span>
</li>
<li id="cite_note-DOI10.1007/s11581-009-0407-4-5"><span class="mw-cite-backlink"><a href="#cite_ref-DOI10.1007/s11581-009-0407-4_5-0">↑</a></span> <span class="reference-text">Mohd Rafie Johan, Tan Kim Han, Abdul Kariem Arof: <i>Growth and sintering effects of hydrated polycrystalline Li<sub>2</sub>WO<sub>4</sub>.</i> In: <i>Ionics.</i> 16, 2010, S. 323, <a href="Digital_Object_Identifier" title="Digital Object Identifier">doi</a>:<span class="uri-handle" style="white-space:nowrap"><a rel="nofollow" class="external text" href="https://doi.org/10.1007/s11581-009-0407-4">10.1007/s11581-009-0407-4</a></span>.</span>
</li>
<li id="cite_note-Evgeni_Tonkov-6"><span class="mw-cite-backlink"><a href="#cite_ref-Evgeni_Tonkov_6-0">↑</a></span> <span class="reference-text">Evgeni Tonkov: <cite style="font-style:italic">High Pressure Phase Transformations A Handbook</cite>. CRC Press, 1992, ISBN 978-2-88124-759-0, <span style="white-space:nowrap">S.<span style="display:inline-block;width:.2em"> </span>534</span> (<a rel="nofollow" class="external text" href="https://books.google.de/books?id=G7HJAOFT7LMC&pg=PA534#v=onepage">eingeschränkte Vorschau</a> in der Google-Buchsuche).<span class="Z3988" title="ctx_ver=Z39.88-2004&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Abook&rfr_id=info:sid/de.wikipedia.org:Lithiumwolframat&rft.au=Evgeni+Tonkov&rft.btitle=High+Pressure+Phase+Transformations+A+Handbook&rft.date=1992&rft.genre=book&rft.isbn=9782881247590&rft.pages=534&rft.pub=CRC+Press" style="display:none"> </span></span>
</li>
<li id="cite_note-DOI10.1016/0022-4596(80)90554-X-7"><span class="mw-cite-backlink"><a href="#cite_ref-DOI10.1016/0022-4596(80)90554-X_7-0">↑</a></span> <span class="reference-text">Hiroyuki Horiuchi, Nobuo Morimoto, Shinobu Yamaoka: <i>The crystal structure of Li<sub>2</sub>WO<sub>4</sub>(IV) and its relation to the wolframite-type structure.</i> In: <i>Journal of Solid State Chemistry.</i> 33, 1980, S. 115, <a href="Digital_Object_Identifier" title="Digital Object Identifier">doi</a>:<span class="uri-handle" style="white-space:nowrap"><a rel="nofollow" class="external text" href="https://doi.org/10.1016/0022-4596%2880%2990554-X">10.1016/0022-4596(80)90554-X</a></span>.</span>
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